Films and getters · Workhorse

Bulk getters: St707 class, ZAO

ZrVFevalues describe: St 707

Vacuum electronics & X-ray sourcesBig science (accelerators, light sources, public fusion)Quantum hardwareVacuum equipment & components

Why it wins

Cartridge and strip getters are the life-of-device vacuum system of sealed tubes and the silent partner of ion pumps in XHV: sealed devices have no pump port, the getter is the pump for 20 years.

Why not the alternative

Nothing else pumps for decades with zero power and zero moving parts.

Watch out

Activation temperature versus package thermal budget.

Properties

The values below are candidate: compiled from the sources named, not yet individually validated. Provisional provenance: SAES Getters datasheets and NEG literature; CERN Accelerator School, vacuum and materials proceedings.

Wet cleaning

Recipenever wet-clean an activated getter; handle the cartridge as delivered, gloves and dry N₂
Forbiddenany solvent or moisture: it consumes capacity irreversibly
Limitcapacity, which cleaning can only spend

Vacuum and outgassing

Outgassing, unbaked (10 h)pumps
Outgassing, bakedpumps
Vapour pressurenone

Temperature

Bake, assembled500 °C
Vacuum degas500 °C
Metallurgical limitactivation 450–500 °C; ZAO activates lower and tolerates air

Thermal

Emissivity0.6

Mechanical

Strengthsintered
Elongationnil
Density6.5 g/cm3

Electrical and magnetic

Relative permeability~1.0

Engineering

Corrosionpyrophoric as fine powder after activation
Joiningsintered on a strip or bolted as a module
Process notescapacity for CO and CO₂ is finite and non-renewable
Availability and costSAES

Outgassing

0 sourced measurements for this card, 2 declared absences. A rate means nothing without the pumping time it was read at, so each one states it or declares it missing. The whole base, filters included, is at /tools/outgassing/.

  • St 101 NEG strip, Zr84-Al16 powder on constantan, 30 mm wide, 100 micron coating both sides (SAES Getters). Getter strip used as a linear pump, activated by resistive heating to 750 C for about half an hour.Section 1 of the source, LEP vacuum system, about 23 of the 27 km. Pumping speed for H2 about 2000 L/s per linear metre. Ultimate pressure about 2e-12 Torr in a LEP dipole chamber after 24 h baking at 150 C, set by the outgassing of CH4 and Ar divided by the pumping speed of a sputter-ion pump of about 50 L/s nominal for a 12 m chamber, with six such pumps on the same chamber, about 5e-13 Torr. Porosity raised from 7 to 13 percent for the LEP delivery. These are pumping speeds and system pressures, not specific outgassing rates. Card assignment to be checked at integration: this strip may belong to a card other than st707-zao.
  • St 707 NEG strip (SAES Getters). Getter strip activated passively during a stainless steel bakeout, around 400 C, no electrical feedthrough required.Section 1 of the source: pumping curves very similar to those of St 101 are obtained after heating at 350 to 400 C. Covering the inner surface of a chamber entirely with St 707 strip, a total NEG pump, gives pumping speeds above 1e4 L/s per linear metre after a 350 C bakeout and pressures below 1e-13 Torr, measured in a 3 m stainless steel tube and stated by the source to be extrapolable to any length because the pump is modular.

Sources: S-BENVENUTI-EPAC1998. Full citations and conditions at the base and in /data/outgassing.json.

Grades

St101 (Zr84-Al16)strip getter heritage (LEP), activation 700 C class
St707 (Zr70-V24.6-Fe5.4)the cartridge workhorse, activation 450 C class
St172sintered porous body pills for sealed devices
ZAOsintered ZrVTiAl, high capacity, low particulation: NEXTorr class pumps
Sources · 1
  1. NEG coatings for synchrotron facilities, review

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Essays

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